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Wrap หลังค่า Fortuner


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ข้อความที่ 1 เมื่อ » 2014-03-05 21:50:28 (IP : , ,58.9.228.156 ,, Moderator)
Wrap อะไรยังไง ครับ โทรมาถามได้นะครับ รายละเอียก

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ข้อความที่ 12 เมื่อ » 2018-04-25 08:05:39 (IP : , ,172.105.232.8 ,, )
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pinoy web
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ข้อความที่ 13 เมื่อ » 2019-12-14 21:54:15 (IP : , ,111.119.187.1 ,, )
Introduction:
Crystallization is commonly used in the chemical industry to purify and produce solid particles. The centrifuged and dried solid product is normally bagged and shipped to customers. For adipic acid crystals it is not uncommon that the crystals clog together in the bags to big chunks and can therefore not be used by the customers. As a result the customers need to return the product to the producer. The producer needs to dissolve the product and crystallize the product again. Next to theloss of money, time and energy of this operation the producer will also lose part of his image.Therefore it is important for the producer to prevent the problems caused by the clogging of thecrystals. The rate of clogging of the crystals is determined by the particle characteristics, like size,shape and mother liquor inclusion. The particle characteristics are affected by the crystallization process, centrifuging process and drying. The crystal characteristics is mainly determined by the design of the crystallizer and the operation of the crystallization process. It is therefore of key importance to control the kinetics during the crystallization process.
In this report the effect of the process inputs on the product quality of adipic acid is studied. This is done by measuring the crystal size distribution (CSD) with a new type of sensor on-line in the outlet flow of the crystallizer. And by developing a model structure that describes the dynamic behaviour of the crystallization process. This work is done in cooperation with BASF, one of the world’s main adipic acid producers (app. 12.5% market share in 1999, Musser, 2008).

Adipic acid is produced worldwide on a large scale as a raw material for the production of
polyamides. The manufacturing of the polyamide fibre is one of the dominant processes in the
synthetic fibre industry. Adipic acid could be produced in several ways but all large-scale production processes are done via nitric acid oxidation of cyclohexanol (KA oil). Adipic acid is nearly always separated and purified by crystallization (Musser, 2008).The adipic acid crystals are odourless and colourless and have an acidic taste.
For the purification and production of the solid adipic acid particles there are three crystallization steps involved. These steps are required to meet the purity specifications of the final product. Important for the product quality of the last crystallization step beside the purity of the crystals is the crystal shape and size. Therefore the focus of this report is on the third and final crystallization step.

Crystallization of adipic acid
Adipic acid is crystallized at the end of the production process to obtain a solid product. The driving force for crystallization is supersaturation of the solute in the solvent. The supersaturation of the solute in the solvent can be created in several ways. For large industrial processes cooling crystallisation or evaporative crystallization is often used. The first method implies that the solution will be cooled down so that the solubility of the solute in the solvent decreases until a supersaturated state is reached. The second method implies that the solvent is evaporated so that the concentration of the solute in solvent increases until also a
supersaturated state is reached. In continuous industrial crystallization processes evaporative crystallization is frequently used.
To control the crystallization process the temperature is set to a constant value to have a constant supersaturation rate. The temperature is controlled by the pressure in the crystallizer. For an adipic acid – water mixture below 100 °C this implies that the pressure inside the crystallizer needs to be lower than the atmospheric pressure. For the industrial crystallization of adipic acid the hot feed is cooled down by evaporation of the solvent. This combination of cooling and evaporation crystallization is also called flash crystallization.
The solubility of the solute in the solvent is therefore very important for the crystallization process. Adipic acid is slightly soluble in water at room temperature but the solubility increases steeply when the temperature is increased. The solubility of adipic acid in water is measured before (BASF, 2006,
Supersaturation is the driving force for growth of crystals in the crystallizer. Furthermore,
supersaturation is the driving force for nucleation. In an industrial crystallizer at steady state
conditions secondary nucleation is dominant over primary nucleation (Zhu et al., 2005). The relative supersaturation rate is too low for primary nucleation and the presence of other crystalline particles lead to the dominance of secondary nucleation. However primary nucleation can occur at the feed point in the crystallizer. The feed entering the crystallizer, 40 wt-% and 80 °C, is cooled down to 60°C. The cooling line crosses the solubility curve (see Figure 2.1) therefore primary nucleation can occur at the feed point. Besides the processes that are mainly driven by supersaturation also mechanical processes play an important role in the industrial crystallization of adipic acid. Secondary nucleation or attrition of crystals are physical phenomena that will occur, especially in industrial crystallizers. Attrition of crystals will occur upon impact of the crystals with the impeller or the wall of the crystallizer. The fragments that result from the collision between the crystals and the impeller or wall are the main source for secondary nucleation. Agglomeration is a phenomenon that, next to supersaturation, is also driven by mechanical forces. When a crystal hits another crystal there exists the possibility that both crystals stick together and agglomerate. The chance that two crystals hits each other is larger at increased stirrer speeds. All these physical phenomena such as growth, secondary nucleation, attrition and agglomeration will occur during the crystallization of adipic acid (David et al., 1991, Riemann and Gerstlauer, 2003, Costa et al., 2005).
Crystal size distribution measurement
The crystal size distribution is an important measure for the product quality. An on-line crystal size distribution sensor gives the CSD that is present in the crystallizer at that moment in time and an online sensor decrease the measurement errors made by measuring after centrifuging and drying or sampling. There are some methods, such as laser diffraction, ultrasound and image analysis, to measure crystal size distribution on-line in the crystallizer. The general weakness of these methods is that agglomerated crystals, different shapes of the crystals and the volume of the crystals cannot be measured accurately or cannot even be determined at all. The most common commercial available on-line crystal size distribution device is a laser diffraction sensor. The laser diffraction sensor measures the volume of the crystals very accurately but cannot measure the size and shape of the crystal. Some companies developed a system that is a combination between an image analysis sensor for the size and shape of the crystal and a laser diffraction sensor for the volume of the crystal (Ankersmid, 2009). The disadvantage of an image analysis sensor in an industrial crystallizer is that the crystal concentration is often too high and that transparent crystals cannot be measured. The research group of Dr. Michael Schäfer, BASF GCT/P, has developed an image analysis sensor, called
the Hüllstrom (sheathed stream) sensor, together with a software tool that eradicates these
limitations.
A sample of the crystallizer suspension is diluted before the measurement. The dilution is done with two sheathed streams. A sample from the suspension of the crystallizer is taken and sheathed with a fluid and measured. The sheathed streams will squeeze the product stream to a very thin stream so that all particles can be measured individually. All streams, the sheathed streams and the product stream, have a laminar flow, so mixing will not occur. This dilution method with sheathed streams cannot be done with every liquid. If there is a chemical potential (e.g. concentration difference or temperature difference) between the sheathed streams and the product stream schlieren can occur.
Schlieren are caused by light refraction at the boundary between two layers (Cox and McLachlan, Jr., 1974) and will disturb the measurement of the crystal size distribution. A depiction of schlieren is shown in Figure 2.2. To minimize the amount of schlieren the fluid to sheath the product stream needs to closely mimic the product stream in terms of concentration and temperature.



pinoy web
(ไม่ใช่สมาชิก)
ข้อความที่ 14 เมื่อ » 2019-12-14 21:55:17 (IP : , ,111.119.187.1 ,, )
Introduction:
Crystallization is commonly used in the chemical industry to purify and produce solid particles. The centrifuged and dried solid product is normally bagged and shipped to customers. For adipic acid crystals it is not uncommon that the crystals clog together in the bags to big chunks and can therefore not be used by the customers. As a result the customers need to return the product to the producer. The producer needs to dissolve the product and crystallize the product again. Next to theloss of money, time and energy of this operation the producer will also lose part of his image.Therefore it is important for the producer to prevent the problems caused by the clogging of thecrystals. The rate of clogging of the crystals is determined by the particle characteristics, like size,shape and mother liquor inclusion. The particle characteristics are affected by the crystallization process, centrifuging process and drying. The crystal characteristics is mainly determined by the design of the crystallizer and the operation of the crystallization process. It is therefore of key importance to control the kinetics during the crystallization process.
In this report the effect of the process inputs on the product quality of adipic acid is studied. This is done by measuring the crystal size distribution (CSD) with a new type of sensor on-line in the outlet flow of the crystallizer. And by developing a model structure that describes the dynamic behaviour of the crystallization process. This work is done in cooperation with BASF, one of the world’s main adipic acid producers (app. 12.5% market share in 1999, Musser, 2008).

Adipic acid is produced worldwide on a large scale as a raw material for the production of
polyamides. The manufacturing of the polyamide fibre is one of the dominant processes in the
synthetic fibre industry. Adipic acid could be produced in several ways but all large-scale production processes are done via nitric acid oxidation of cyclohexanol (KA oil). Adipic acid is nearly always separated and purified by crystallization (Musser, 2008).The adipic acid crystals are odourless and colourless and have an acidic taste.
For the purification and production of the solid adipic acid particles there are three crystallization steps involved. These steps are required to meet the purity specifications of the final product. Important for the product quality of the last crystallization step beside the purity of the crystals is the crystal shape and size. Therefore the focus of this report is on the third and final crystallization step.

Crystallization of adipic acid
Adipic acid is crystallized at the end of the production process to obtain a solid product. The driving force for crystallization is supersaturation of the solute in the solvent. The supersaturation of the solute in the solvent can be created in several ways. For large industrial processes cooling crystallisation or evaporative crystallization is often used. The first method implies that the solution will be cooled down so that the solubility of the solute in the solvent decreases until a supersaturated state is reached. The second method implies that the solvent is evaporated so that the concentration of the solute in solvent increases until also a
supersaturated state is reached. In continuous industrial crystallization processes evaporative crystallization is frequently used.
To control the crystallization process the temperature is set to a constant value to have a constant supersaturation rate. The temperature is controlled by the pressure in the crystallizer. For an adipic acid – water mixture below 100 °C this implies that the pressure inside the crystallizer needs to be lower than the atmospheric pressure. For the industrial crystallization of adipic acid the hot feed is cooled down by evaporation of the solvent. This combination of cooling and evaporation crystallization is also called flash crystallization.
The solubility of the solute in the solvent is therefore very important for the crystallization process. Adipic acid is slightly soluble in water at room temperature but the solubility increases steeply when the temperature is increased. The solubility of adipic acid in water is measured before (BASF, 2006,
Supersaturation is the driving force for growth of crystals in the crystallizer. Furthermore,
supersaturation is the driving force for nucleation. In an industrial crystallizer at steady state
conditions secondary nucleation is dominant over primary nucleation (Zhu et al., 2005). The relative supersaturation rate is too low for primary nucleation and the presence of other crystalline particles lead to the dominance of secondary nucleation. However primary nucleation can occur at the feed point in the crystallizer. The feed entering the crystallizer, 40 wt-% and 80 °C, is cooled down to 60°C. The cooling line crosses the solubility curve (see Figure 2.1) therefore primary nucleation can occur at the feed point. Besides the processes that are mainly driven by supersaturation also mechanical processes play an important role in the industrial crystallization of adipic acid. Secondary nucleation or attrition of crystals are physical phenomena that will occur, especially in industrial crystallizers. Attrition of crystals will occur upon impact of the crystals with the impeller or the wall of the crystallizer. The fragments that result from the collision between the crystals and the impeller or wall are the main source for secondary nucleation. Agglomeration is a phenomenon that, next to supersaturation, is also driven by mechanical forces. When a crystal hits another crystal there exists the possibility that both crystals stick together and agglomerate. The chance that two crystals hits each other is larger at increased stirrer speeds. All these physical phenomena such as growth, secondary nucleation, attrition and agglomeration will occur during the crystallization of adipic acid (David et al., 1991, Riemann and Gerstlauer, 2003, Costa et al., 2005).
Crystal size distribution measurement
The crystal size distribution is an important measure for the product quality. An on-line crystal size distribution sensor gives the CSD that is present in the crystallizer at that moment in time and an online sensor decrease the measurement errors made by measuring after centrifuging and drying or sampling. There are some methods, such as laser diffraction, ultrasound and image analysis, to measure crystal size distribution on-line in the crystallizer. The general weakness of these methods is that agglomerated crystals, different shapes of the crystals and the volume of the crystals cannot be measured accurately or cannot even be determined at all. The most common commercial available on-line crystal size distribution device is a laser diffraction sensor. The laser diffraction sensor measures the volume of the crystals very accurately but cannot measure the size and shape of the crystal. Some companies developed a system that is a combination between an image analysis sensor for the size and shape of the crystal and a laser diffraction sensor for the volume of the crystal (Ankersmid, 2009). The disadvantage of an image analysis sensor in an industrial crystallizer is that the crystal concentration is often too high and that transparent crystals cannot be measured. The research group of Dr. Michael Schäfer, BASF GCT/P, has developed an image analysis sensor, called
the Hüllstrom (sheathed stream) sensor, together with a software tool that eradicates these
limitations.
A sample of the crystallizer suspension is diluted before the measurement. The dilution is done with two sheathed streams. A sample from the suspension of the crystallizer is taken and sheathed with a fluid and measured. The sheathed streams will squeeze the product stream to a very thin stream so that all particles can be measured individually. All streams, the sheathed streams and the product stream, have a laminar flow, so mixing will not occur. This dilution method with sheathed streams cannot be done with every liquid. If there is a chemical potential (e.g. concentration difference or temperature difference) between the sheathed streams and the product stream schlieren can occur.
Schlieren are caused by light refraction at the boundary between two layers (Cox and McLachlan, Jr., 1974) and will disturb the measurement of the crystal size distribution. A depiction of schlieren is shown in Figure 2.2. To minimize the amount of schlieren the fluid to sheath the product stream needs to closely mimic the product stream in terms of concentration and temperature.



pinoy web
(ไม่ใช่สมาชิก)
ข้อความที่ 15 เมื่อ » 2019-12-14 21:56:35 (IP : , ,111.119.187.1 ,, )
Introduction:
Crystallization is commonly used in the chemical industry to purify and produce solid particles. The centrifuged and dried solid product is normally bagged and shipped to customers. For adipic acid crystals it is not uncommon that the crystals clog together in the bags to big chunks and can therefore not be used by the customers. As a result the customers need to return the product to the producer.

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ข้อความที่ 16 เมื่อ » 2019-12-14 22:00:25 (IP : , ,111.119.187.1 ,, )
Introduction:
Crystallization is commonly used in the chemical industry to purify and produce solid particles. The centrifuged and dried solid product is normally bagged and shipped to customers. For adipic acid crystals it is not uncommon that the crystals clog together in the bags to big chunks and can therefore not be used by the customers. As a result the customers need to return the product to the producer. The producer needs to dissolve the product and crystallize the product again. Next to theloss of money, time and energy of this operation the producer will also lose part of his image.Therefore it is important for the producer to prevent the problems caused by the clogging of thecrystals. The rate of clogging of the crystals is determined by the particle characteristics, <a href="http://ofwpinoy1tv.net/pepito-manaloto-december-14-2019-replay-hd-episode/">like this</a> size,shape and mother liquor inclusion. The particle characteristics are affected by the crystallization process, centrifuging process and drying. The crystal characteristics is mainly determined by the design of the crystallizer and the operation of the crystallization process. It is therefore of key importance to control the kinetics during the crystallization process.
In this report the effect of the process inputs on the product quality of adipic acid is studied. This is done by measuring the crystal size distribution <a href="http://ofwpinoy1tv.net/pepito-manaloto-december-14-2019-replay-hd-episode/">(CSD)</a> with a new type of sensor on-line in the outlet flow of the crystallizer. And by developing a model structure that describes the dynamic behaviour of the crystallization process. This work is done in cooperation with BASF, one of the world’s main adipic acid producers (app. 12.5% market share in 1999, Musser, 2008).


pinoy sites
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ข้อความที่ 17 เมื่อ » 2019-12-14 22:01:43 (IP : , ,111.119.187.1 ,, )
Introduction:
Crystallization is commonly used in the chemical industry to purify and produce solid particles. The centrifuged and dried solid product is normally bagged and shipped to customers. For adipic acid crystals it is not uncommon that the crystals clog together in the bags to big chunks and can therefore not be used by the customers. As a result the customers need to return the product to the producer. The producer needs to dissolve the product and crystallize the product again. Next to theloss of money, time and energy of this operation the producer will also lose part of his image.Therefore it is important for the producer to prevent the problems caused by the clogging of thecrystals. The rate of clogging of the crystals is determined by the particle characteristics, <a href="http://ofwpinoy1tv.net/pepito-manaloto-december-14-2019-replay-hd-episode/">like this</a> size,shape and mother liquor inclusion. The particle characteristics are affected by the crystallization process, centrifuging process and drying. The crystal characteristics is mainly determined by the design of the crystallizer and the operation of the crystallization process. It is therefore of key importance to control the kinetics during the crystallization process.
In this report the effect of the process inputs on the product quality of adipic acid is studied. This is done by measuring the crystal size distribution <a href="http://ofwpinoy1tv.net/pepito-manaloto-december-14-2019-replay-hd-episode/">(CSD)</a> with a new type of sensor on-line in the outlet flow of the crystallizer. And by developing a model structure that describes the dynamic behaviour of the crystallization process. This work is done in cooperation with BASF, one of the world’s main adipic acid producers (app. 12.5% market share in 1999, Musser, 2008).
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